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Influence of spark plasma sintering and baghdadite powder on mechanical properties of hydroxyapatite

机译:火花等离子体烧结和巴格达粉末对羟基磷灰石力学性能的影响

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摘要

Since hydroxyapatite-based materials have similar composition and crystallinity as natural calcified tissues, can be used for bone/tissue engineering. In the present study a novel nanocomposite based on bioceramics such as Natural Hydroxyapatite (NHA) and Baghdadite (BAG), was sintered by spark plasma sintering (SPS) technique. The prepared composite was characterized using scanning electron microscopy (SEM), X-ray diffractometer (XRD) and Brunauer-Emmett-Teller (BET) techniques. The porosity of the samples was measured by Archimedes method. The cold crushing strength (CCS) test was applied to evaluate their mechanical properties. Our results demonstrated that NHA-30wt. %BAG nanocomposite specimens have the lower CCS in comparison with other examined composites. Consequently, NHA/BAG samples exhibited acceptable mechanical properties and could be suitable candidates for bone tissue engineering applications especially orthopaedic fields.
机译:由于基于羟基磷灰石的材料具有与天然钙化组织相似的组成和结晶度,因此可用于骨骼/组织工程。在本研究中,通过火花等离子体烧结(SPS)技术烧结了一种基于生物陶瓷的新型纳米复合材料,例如天然羟基磷灰石(NHA)和巴格达特(BAG)。使用扫描电子显微镜(SEM),X射线衍射仪(XRD)和Brunauer-Emmett-Teller(BET)技术对制备的复合材料进行表征。样品的孔隙率通过阿基米德法测量。应用冷压强度(CCS)测试来评估其机械性能。我们的结果表明,NHA-30wt。与其他检查的复合材料相比,%BAG纳米复合材料样品的CCS较低。因此,NHA / BAG样品表现出可接受的机械性能,并且可能适合用于骨组织工程应用,尤其是整形外科领域。

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